Note: Contamination-free loading of lithium metal into a nozzle source

Rev Sci Instrum. 2016 Jun;87(6):066105. doi: 10.1063/1.4953918.

Abstract

This note describes a system for transferring a load of high purity lithium metal into a molecular or cluster beam source. A hot loading vessel is thoroughly baked out while empty and overpressured with argon. A clean Li rod is then dropped in through a long narrow tube. The thoroughly degassed interior of the vessel and the rapid melting of the inserted rod facilitate contamination-free transfer of the highly reactive liquid metal into the source oven.