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, 55 (Pt 7), 1329-34

Macromolecular Crystal Annealing: Evaluation of Techniques and Variables

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Macromolecular Crystal Annealing: Evaluation of Techniques and Variables

J M Harp et al. Acta Crystallogr D Biol Crystallogr.

Abstract

Additional examples of successful application of macromolecular crystal annealing are presented. A qualitative evaluation of variables related to the annealing process was conducted using a variety of macromolecular crystals to determine in which cases parameters may be varied and in which cases the original macromolecular crystal annealing protocol is preferred. A hypothesis is presented relating the solvent content of the crystal to the specific protocol necessary for the successful application of annealing.

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