The influence of clinically induced variability on the distribution of compressive fracture strengths of a hand-mixed zinc phosphate dental cement

Dent Mater. 1999 Mar;15(2):87-97. doi: 10.1016/s0109-5641(99)00018-4.

Abstract

Objectives: Conventional approaches to comparing dental cements use standard property tests under manufacturers' specified conditions. Zinc phosphate cements are supplied in powder/liquid form and manipulation frequently involves mixing the components by eye so a range of mixing ratios will inevitably occur in practice. Unfortunately, the physical, chemical, biological and mechanical properties of cements are known to be dependent on the mixing ratio.

Methods: Forty dental nurses prepared a series of three cement samples to a luting consistency they considered acceptable for use in practice.

Results: It was found that each dental nurse produced consistent cement mixes, although, the mixing ratios varied from 1.7 to 3.2 g/ml between nurses. The mean compressive strength, standard deviation and associated Weibull Moduli (m) of the cements were determined as a function of this mixing ratio range and showed considerable variation ranging from 33.5 +/- 3.2 MPa (m = 11.0) at 1.7 g/ml to 71.4 +/- 8.4 MPa (m = 8.6) at 2.6 g/ml and 42.5 +/- 10.0 MPa (m = 5.0) at 3.2 g/ml.

Significance: An analytical approach was adopted which facilitated an integrated analysis of the mixing ratio variability with the strength data. It was found for the test group of dental nurses that 25% of cement mixes produced would have achieved strengths below 40 MPa whilst strengths below the standard value were produced in at least 70% of mixes. These results indicate that a simple analysis of the properties of cements manipulated under optimum conditions, provides little information on the material characteristics obtained in practice because of clinically induced variability.

MeSH terms

  • Analysis of Variance
  • Compressive Strength
  • Least-Squares Analysis
  • Materials Testing
  • Survival Analysis
  • Technology, Dental
  • Zinc Phosphate Cement / chemistry*

Substances

  • Zinc Phosphate Cement