Structural studies of lysyl-tRNA synthetase: conformational changes induced by substrate binding

Biochemistry. 2000 Oct 24;39(42):12853-61. doi: 10.1021/bi001487r.

Abstract

Lysyl-tRNA synthetase is a member of the class II aminoacyl-tRNA synthetases and catalyses the specific aminoacylation of tRNA(Lys). The crystal structure of the constitutive lysyl-tRNA synthetase (LysS) from Escherichia coli has been determined to 2.7 A resolution in the unliganded form and in a complex with the lysine substrate. A comparison between the unliganded and lysine-bound structures reveals major conformational changes upon lysine binding. The lysine substrate is involved in a network of hydrogen bonds. Two of these interactions, one between the alpha-amino group and the carbonyl oxygen of Gly 216 and the other between the carboxylate group and the side chain of Arg 262, trigger a subtle and complicated reorganization of the active site, involving the ordering of two loops (residues 215-217 and 444-455), a change in conformation of residues 393-409, and a rotation of a 4-helix bundle domain (located between motif 2 and 3) by 10 degrees. The result of these changes is a closing up of the active site upon lysine binding.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adenosine Triphosphate / chemistry
  • Adenosine Triphosphate / metabolism
  • Binding Sites
  • Crystallization
  • Crystallography, X-Ray
  • Escherichia coli / enzymology
  • Isoenzymes / chemistry
  • Isoenzymes / metabolism
  • Lysine / chemistry
  • Lysine / metabolism
  • Lysine-tRNA Ligase / chemistry*
  • Lysine-tRNA Ligase / metabolism
  • Models, Molecular
  • Peptide Fragments / chemistry
  • Peptide Fragments / metabolism
  • Protein Conformation
  • Protein Structure, Tertiary
  • RNA, Transfer / chemistry
  • RNA, Transfer / metabolism
  • Substrate Specificity

Substances

  • Isoenzymes
  • Peptide Fragments
  • Adenosine Triphosphate
  • RNA, Transfer
  • Lysine-tRNA Ligase
  • Lysine

Associated data

  • PDB/1BBU
  • PDB/1BBW