The effect of thermocycling on the fracture toughness and hardness of core buildup materials

J Prosthet Dent. 2001 Nov;86(5):474-80. doi: 10.1067/mpr.2001.120110.

Abstract

Statement of problem: Thermocycling has been shown to cause surface degradation of many dental materials, but its effect on the fracture toughness and hardness of direct core buildup materials is unknown.

Purpose: This study was designed to determine the effect of thermocycling on the fracture toughness and hardness of 5 core buildup materials.

Material and methods: Fifteen specimens were prepared from each of the following materials: Fluorocore, VariGlass VLC, Valiant PhD, Vitremer, and Chelon-Silver. American Standard for Testing Materials guidelines for single-edge notch, bar-shaped specimens were used. Ten specimens of each material were thermocycled for 2000 cycles; the other 5 specimens were not thermocycled. All specimens were subjected to 3-point bending in a universal testing machine. The load at fracture was recorded, and the fracture toughness (K(IC)) was calculated. Barcol hardness values were also determined. Data were analyzed with 1-way analysis of variance and compared with the Tukey multiple range test (P<.05). Pearson's correlation coefficient was also calculated to measure the association between fracture toughness and hardness.

Results: Fluorocore had the highest thermocycled mean K(IC) and Valiant PhD the highest non-thermocycled K(IC). Chelon-Silver demonstrated the lowest mean K(IC) both before and after thermocycling. One-way analysis of variance demonstrated significant differences between conditions, and the Tukey test showed significant differences (P<.05) between materials for both conditions. Most specimens also showed significant hardness differences between conditions. Pearson's correlation coefficient indicated only a mild-to-moderate correlation between hardness and fracture toughness.

Conclusion: Within the limitations of this study, the thermocycling process negatively affected the fracture toughness and hardness of the core buildup materials tested.

Publication types

  • Comparative Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acrylic Resins / chemistry
  • Analysis of Variance
  • Cermet Cements / chemistry
  • Composite Resins / chemistry
  • Confidence Intervals
  • Dental Alloys / chemistry
  • Dental Materials / chemistry*
  • Dental Stress Analysis / instrumentation
  • Fluorides, Topical / chemistry
  • Glass Ionomer Cements / chemistry
  • Hardness
  • Humans
  • Materials Testing
  • Pliability
  • Post and Core Technique / instrumentation*
  • Resin Cements / chemistry
  • Silver Compounds / chemistry
  • Statistics as Topic
  • Stress, Mechanical
  • Surface Properties
  • Thermodynamics

Substances

  • Acrylic Resins
  • Cermet Cements
  • Composite Resins
  • Dental Alloys
  • Dental Materials
  • Fluorides, Topical
  • FluoroCore
  • Glass Ionomer Cements
  • Resin Cements
  • Silver Compounds
  • VariGlass VLC
  • Vitremer
  • Chelon Silver
  • Valiant PhD