The nature of the di-iron site in the bacterioferritin from Desulfovibrio desulfuricans

Nat Struct Biol. 2003 Apr;10(4):285-90. doi: 10.1038/nsb909.

Abstract

The first crystal structure of a native di-iron center in an iron-storage protein (bacterio)ferritin is reported. The protein, isolated from the anaerobic bacterium Desulfovibrio desulfuricans, has the unique property of having Fe-coproporphyrin III as its heme cofactor. The three-dimensional structure of this bacterioferritin was determined in three distinct catalytic/redox states by X-ray crystallography (at 1.95, 2.05 and 2.35 A resolution), corresponding to different intermediates of the di-iron ferroxidase site. Conformational changes associated with these intermediates support the idea of a route for iron entry into the protein shell through a pore that passes through the di-iron center. Molecular surface and electrostatic potential calculations also suggest the presence of another ion channel, distant from the channels at the three- and four-fold axes proposed as points of entry for the iron atoms.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Bacterial Proteins*
  • Binding Sites
  • Ceruloplasmin / chemistry
  • Crystallography, X-Ray
  • Cytochrome b Group / chemistry*
  • Desulfovibrio / chemistry
  • Ferritins / chemistry*
  • Heme / chemistry
  • Ion Channels / chemistry
  • Iron / chemistry
  • Models, Molecular
  • Oxidation-Reduction
  • Protein Conformation
  • Protein Structure, Quaternary
  • Protein Subunits
  • Static Electricity

Substances

  • Bacterial Proteins
  • Cytochrome b Group
  • Ion Channels
  • Protein Subunits
  • Heme
  • Ferritins
  • bacterioferritin
  • Iron
  • Ceruloplasmin

Associated data

  • PDB/1NF4
  • PDB/1NF6
  • PDB/1NFV