Engineering of pyranose 2-oxidase from Peniophora gigantea towards improved thermostability and catalytic efficiency

Appl Microbiol Biotechnol. 2005 Jun;67(5):654-63. doi: 10.1007/s00253-004-1813-1. Epub 2005 Jan 20.

Abstract

To improve the stability and catalytic efficiency of pyranose 2-oxidase (P2Ox) by molecular enzyme evolution, we cloned P2Ox cDNA by RACE-PCR from a cDNA library derived from the basidiomycete Peniophora gigantea. The P2Ox gene was expressed in Escherichia coli BL21(DE3), yielding an intracellular and enzymatically active P2OxB with a volumetric yield of 500 units/l. Site-directed mutagenesis was employed to construct the P2Ox variant E540K (termed P2OxB1), which exhibited increased thermo- and pH-stability compared with the wild type, concomitantly with increased catalytic efficiencies (k(cat)/K(m)) for D-xylose and L-sorbose. P2OxB1 was provided with a C-terminal His(6)-tag (termed P2OxB1H) and subjected to directed evolution using error-prone PCR. Screening based on a chromogenic assay yielded the new P2Ox variant K312E (termed P2OxB2H) that showed significant improvements with respect to k(cat)/K(m) for D-glucose (5.3-fold), methyl-beta-D-glucoside (2.0-fold), D-galactose (4.8-fold), D-xylose (59.9-fold), and L-sorbose (69.0-fold), compared with wild-type P2Ox. The improved catalytic performance of P2OxB2H was demonstrated by bioconversions of L-sorbose that initially was a poor substrate for wild-type P2Ox. This is the first report on the improvement of a pyranose 2-oxidase by a dual approach of site-directed mutagenesis and directed evolution, and the application of the engineered P2Ox in bioconversions.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Amino Acid Substitution
  • Basidiomycota / enzymology*
  • Carbohydrate Dehydrogenases / chemistry*
  • Carbohydrate Dehydrogenases / genetics
  • Carbohydrate Dehydrogenases / metabolism*
  • Cloning, Molecular
  • DNA, Fungal / chemistry
  • DNA, Fungal / genetics
  • Directed Molecular Evolution
  • Enzyme Stability / genetics
  • Escherichia coli / genetics
  • Escherichia coli / metabolism
  • Fungal Proteins / chemistry*
  • Fungal Proteins / genetics
  • Fungal Proteins / metabolism*
  • Galactose / metabolism
  • Gene Expression
  • Glucose / metabolism
  • Hydrogen-Ion Concentration
  • Methylglucosides / metabolism
  • Molecular Sequence Data
  • Mutagenesis, Site-Directed
  • Mutation, Missense
  • Polymerase Chain Reaction
  • Protein Engineering*
  • Recombinant Proteins / genetics
  • Recombinant Proteins / metabolism
  • Sequence Analysis, DNA
  • Sorbose / metabolism
  • Temperature
  • Xylose / metabolism

Substances

  • DNA, Fungal
  • Fungal Proteins
  • Methylglucosides
  • Recombinant Proteins
  • methylglucoside
  • Xylose
  • Carbohydrate Dehydrogenases
  • poxB protein, Phlebiopsis gigantea
  • Glucose
  • Sorbose
  • Galactose

Associated data

  • GENBANK/AY370876