Specific epitopes of domains II and III of Bacillus thuringiensis Cry1Ab toxin involved in the sequential interaction with cadherin and aminopeptidase-N receptors in Manduca sexta

J Biol Chem. 2006 Nov 10;281(45):34032-9. doi: 10.1074/jbc.M604721200. Epub 2006 Sep 12.

Abstract

The Bacillus thuringiensis Cry toxins are specific to different insects. In Manduca sexta cadherin (Bt-R1) and aminopeptidase-N (APN) proteins are recognized as Cry1A receptors. Previous work showed that Cry1Ab binds to Bt-R1 promoting the formation of a pre-pore oligomer that binds to APN leading to membrane insertion. In this work we characterized the binding epitopes involved in the sequential interaction of Cry1Ab with Bt-R1 and APN. A Cry1Ab immune M13 phage repertoire was constructed using antibody gene transcripts of bone marrow or spleen from a rabbit immunized with Cry1Ab. We identified antibodies that recognize domain II loop 3 (scFvL3-3) or beta16-beta22 (scFvM22) in domain III. Enzyme-linked immunosorbent assay and toxin overlay binding competition assays in the presence of scFvL3-3, scFvM22, or synthetic peptides showed that domain II loop 3 is an important epitope for interaction with Bt-R1 receptor, whereas domain III beta16 is involved in the interaction with APN. Both scFvL3-3 and scFvM22 lowered the toxicity of Cry1Ab to M. sexta larvae indicating that interaction with both receptors is important for in vivo toxicity. scFvL3-3 and anti-loop2 scFv (scFv73) promoted the formation of the pre-pore oligomer in contrast to scFvM22. In addition, scFvL3-3 and scFv73 preferentially recognized the monomeric toxin rather than the pre-pore suggesting a conformational change in domain II loops upon oligomerization. These results indicate for the first time that both receptor molecules participate in Cry1Ab toxin action in vivo: first the monomeric toxin binds to Bt-R1 through loops 2 and 3 of domain II promoting the formation of the pre-pore inducing some structural changes, then the pre-pore interacts with APN through beta-16 of domain III promoting membrane insertion and cell death.

Publication types

  • Research Support, Non-U.S. Gov't
  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Animals
  • Bacillus thuringiensis / chemistry*
  • Bacillus thuringiensis Toxins
  • Bacterial Proteins / chemistry
  • Bacterial Proteins / metabolism*
  • Bacterial Proteins / toxicity
  • Bacterial Toxins / chemistry
  • Bacterial Toxins / metabolism*
  • Bacterial Toxins / toxicity
  • CD13 Antigens / metabolism*
  • Cadherins / metabolism*
  • Endotoxins / chemistry
  • Endotoxins / metabolism*
  • Endotoxins / toxicity
  • Epitopes / analysis
  • Epitopes / chemistry
  • Hemolysin Proteins / chemistry
  • Hemolysin Proteins / metabolism*
  • Hemolysin Proteins / toxicity
  • Immunization
  • Immunoglobulin Variable Region / immunology
  • Immunoglobulin Variable Region / metabolism
  • Insecticides / chemistry
  • Insecticides / metabolism*
  • Insecticides / toxicity
  • Manduca / metabolism*
  • Microvilli / metabolism
  • Peptide Library
  • Peptides / chemistry
  • Peptides / immunology
  • Peptides / metabolism
  • Pest Control, Biological
  • Protein Binding
  • Rabbits
  • Receptors, Cell Surface / metabolism*
  • Recombinant Proteins / chemistry
  • Recombinant Proteins / metabolism

Substances

  • Bacillus thuringiensis Toxins
  • Bacterial Proteins
  • Bacterial Toxins
  • Cadherins
  • Endotoxins
  • Epitopes
  • Hemolysin Proteins
  • Immunoglobulin Variable Region
  • Insecticides
  • Peptide Library
  • Peptides
  • Receptors, Cell Surface
  • Recombinant Proteins
  • insecticidal crystal protein, Bacillus Thuringiensis
  • CD13 Antigens