Optimization of paper bridge loading for 2-DE analysis in the basic pH region: application to the mitochondrial subproteome

Proteomics. 2006 Nov;6(21):5683-7. doi: 10.1002/pmic.200600267.

Abstract

Separation of basic proteins with 2-DE presents technical challenges involving protein precipitation, load limitations, and streaking. Cardiac mitochondria are enriched in basic proteins and difficult to resolve by 2-DE. We investigated two methods, cup and paper bridge, for sample loading of this subproteome into the basic range (pH 6-11) gels. Paper bridge loading consistently produced improved resolution of both analytical and preparative protein loads. A unique benefit of this technique is that proteins retained in the paper bridge after loading basic gels can be reloaded onto lower pH gradients (pH 4-7), allowing valued samples to be analyzed on multiple pH ranges.

Publication types

  • Comparative Study
  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Electrophoresis, Gel, Two-Dimensional / methods*
  • Hydrogen-Ion Concentration
  • Mice
  • Mitochondria, Heart / chemistry*
  • Peptide Mapping
  • Proteome / analysis*
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization
  • Submitochondrial Particles / chemistry*

Substances

  • Proteome