The leaves of CUNILA SPICATA Benth. (Lamiaceae) yielded a monoterpene diacetate called iso-rosiridol diacetate ( 1) and two isomeric hydroperoxymonoterpenes ( 2, 3) as well as beta-sitosterol, phytol, cadinol, linalool, dihydrocarveol, geranyl and neryl acetate. Structure elucidation was done by high-field NMR-techniques.