Broadband carbon-13 correlation spectra of microcrystalline proteins in very high magnetic fields

Markus Weingarth; Geoffrey Bodenhausen; Piotr Tekely

doi:10.1021/ja9036143

Broadband carbon-13 correlation spectra of microcrystalline proteins in very high magnetic fields

J Am Chem Soc. 2009 Oct 7;131(39):13937-9. doi: 10.1021/ja9036143.

Authors

Markus Weingarth¹, Geoffrey Bodenhausen, Piotr Tekely

Affiliation

¹ Département de Chimie, Ecole Normale Supérieure, 24 rue Lhomond, 75231 Paris cedex 05, France.

PMID: 19743847
DOI: 10.1021/ja9036143

Abstract

PARIS recoupling irradiation, despite a low rf amplitude, can promote efficient magnetization transfer during solid-state NMR experiments at 900 MHz over a wide range of differences in isotropic chemical shifts in microcrystalline proteins.

Publication types

Research Support, Non-U.S. Gov't

MeSH terms

Carbon Isotopes*
Crystallization
Magnetics
Nuclear Magnetic Resonance, Biomolecular / methods*
Proteins / chemistry*

Substances

Carbon Isotopes
Proteins