The analytical specificity of human chorionic gonadotropin assays determined using WHO International Reference Reagents

Clin Chim Acta. 2010 Jan;411(1-2):81-5. doi: 10.1016/j.cca.2009.10.009. Epub 2009 Oct 17.

Abstract

Background: Human chorionic gonadotropin (hCG) is a heterodimeric glycoprotein hormone with considerable molecular heterogeneity. There is uncertainty regarding which hCG variants are detected by different hCG assays. The analytical specificity of 8 hCG assays was investigated.

Methods: WHO International Reference Reagents for hCG, nicked hCG (hCGn), beta subunit (hCGbeta), nicked beta subunit (hCGbetan), and beta core fragment (hCGbetacf) were individually added to hCG-free human serum. Specimens were analyzed with 8 commercially available hCG assays. Equimolar detection of hCG variants was defined as a recovery of 90-110%.

Results: All assays detected hCG and hCGn with mean recoveries of 98.3 and 94.6%, respectively. Seven assays detected hCGbeta (mean recovery 103.8%) but with high variation, and equimolar detection was observed only in four. The mean recovery of hCGbetan was 85.5% but was highly variable with only two assays showing equimolar detection. With a mean recovery of 53.4%, two assays detected hCGbetacf and both underestimated it considerably. Information provided by the assay manufacturer regarding hCG variant analytical specificity was inadequate or unclear in 75% of the assays.

Conclusions: hCG assays vary considerably in their ability to detect different hCG variants. Manufacturers of hCG assays should clearly indicate the hCG variant specificity of their reagent systems.

MeSH terms

  • Chorionic Gonadotropin / analysis*
  • Chorionic Gonadotropin / blood
  • Chorionic Gonadotropin / standards
  • Chorionic Gonadotropin / urine
  • Humans
  • Indicators and Reagents / chemistry*
  • Reference Standards
  • Reproducibility of Results
  • World Health Organization

Substances

  • Chorionic Gonadotropin
  • Indicators and Reagents