Green synthesis and characterization of gelatin-based and sugar-reduced silver nanoparticles

Int J Nanomedicine. 2011:6:569-74. doi: 10.2147/IJN.S16867. Epub 2011 Mar 17.

Abstract

Silver nanoparticles (Ag-NPs) have been successfully prepared with simple and "green" synthesis method by reducing Ag(+) ions in aqueous gelatin media with and in the absence of glucose as a reducing agent. In this study, gelatin was used for the first time as a reducing and stabilizing agent. The effect of temperature on particle size of Ag-NPs was also studied. It was found that with increasing temperature the size of nanoparticles is decreased. It was found that the particle size of Ag-NPs obtained in gelatin solutions is smaller than in gelatin-glucose solutions, which can be related to the rate of reduction reaction. X-ray diffraction, ultraviolet-visible spectra, transmission electron microscopy, and atomic force microscopy revealed the formation of monodispersed Ag-NPs with a narrow particle size distribution.

Keywords: UV-vis spectra; gelatin; glucose; green method; silver nanoparticles.

MeSH terms

  • Excipients / chemistry
  • Gelatin / chemistry*
  • Glucose / chemistry*
  • Green Chemistry Technology / methods*
  • Metal Nanoparticles / chemistry*
  • Microscopy, Atomic Force
  • Microscopy, Electron, Transmission
  • Particle Size
  • Silver / chemistry*
  • Spectrophotometry, Ultraviolet
  • Temperature
  • X-Ray Diffraction

Substances

  • Excipients
  • Silver
  • Gelatin
  • Glucose