Pressurized fluid extraction of essential oil from Lavandula hybrida using a modified supercritical fluid extractor and a central composite design for optimization

J Sep Sci. 2012 Jun;35(12):1479-85. doi: 10.1002/jssc.201200043.

Abstract

Essential oil components were extracted from lavandin (Lavandula hybrida) flowers using pressurized fluid extraction. A central composite design was used to optimize the effective extraction variables. The chemical composition of extracted samples was analyzed by a gas chromatograph-flame ionization detector column. For achieving 100% extraction yield, the temperature, pressure, extraction time, and the solvent flow rate were adjusted at 90.6°C, 63 bar, 30.4 min, and 0.2 mL/min, respectively. The results showed that pressurized fluid extraction is a practical technique for separation of constituents such as 1,8-cineole (8.1%), linalool (34.1%), linalyl acetate (30.5%), and camphor (7.3%) from lavandin to be applied in the food, fragrance, pharmaceutical, and natural biocides industries.

Publication types

  • Evaluation Study
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Chromatography, Gas
  • Chromatography, Supercritical Fluid / instrumentation
  • Chromatography, Supercritical Fluid / methods*
  • Flowers / chemistry
  • Lavandula / chemistry*
  • Oils, Volatile / analysis
  • Oils, Volatile / isolation & purification*
  • Plant Extracts / analysis
  • Plant Extracts / isolation & purification*

Substances

  • Oils, Volatile
  • Plant Extracts