Using light to covalently immobilize and pattern nanoparticles onto surfaces

Langmuir. 2012 Jul 24;28(29):10934-41. doi: 10.1021/la302113k. Epub 2012 Jul 13.

Abstract

There is considerable current interest in developing methods to integrate nanoparticles into optical, electronic, and biological systems due to their unique size-dependent properties and controllable shape. We report herein a versatile new approach for covalent immobilization of nanoparticles onto substrates modified with photoactive, phthalimide-functional, self-assembled monolayers. Upon illumination with UV radiation, the phthalimide group abstracts a hydrogen atom from a neighboring organic molecule, leading to radical-based photografting reactions. The approach is potentially "universal" since virtually any polymeric or organic-inorganic hybrid nanoparticle can be covalently immobilized in this fashion. Because grafting is confined to illuminated regions that undergo photoexcitation, masking provides a simple and direct method for nanoparticle patterning. To illustrate the technique, nanoparticles formed from diblock copolymers of poly(styrene-b-polyethylene oxide) and laden with Hostasol Red dye are photografted and patterned onto glass and silicon substrates modified with photoactive phthalimide-silane self-assembled monolayers. Atomic force microscopy and X-ray photoelectron spectroscopy are applied to characterize the grafted nanoparticle films while confocal fluorescence microscopy is used to image patterned nanoparticle deposition.

Publication types

  • Research Support, U.S. Gov't, Non-P.H.S.

MeSH terms

  • Congo Red / chemistry
  • Molecular Structure
  • Nanoparticles / chemistry*
  • Particle Size
  • Phthalimides / chemistry
  • Polyethylene Glycols / chemistry
  • Polystyrenes / chemistry
  • Silanes / chemistry
  • Silicon / chemistry
  • Surface Properties
  • Ultraviolet Rays*

Substances

  • Phthalimides
  • Polystyrenes
  • Silanes
  • polystyrene-b-poly(ethylene oxide)
  • phthalimide
  • Congo Red
  • Polyethylene Glycols
  • Silicon