Expression, purification, crystallization and preliminary crystallographic analysis of hepatitis B virus core protein dimerized via a peptide linker containing an EGFP insertion

Acta Crystallogr Sect F Struct Biol Cryst Commun. 2013 Aug;69(Pt 8):942-5. doi: 10.1107/S1744309113019957. Epub 2013 Jul 27.

Abstract

Virus-like particles (VLPs) have many potentially useful applications. The core proteins of human hepatitis B virus self-assemble into icosahedral VLPs. As previously reported, core protein dimers (CPDs), produced by connecting two core proteins via a peptide linker, can also assemble into VLPs. CPDs in which heterologous proteins were connected to the C-terminus (CPD1) were found to rearrange into symmetrical octahedra during crystallization. In this study, a heterologous protein was inserted into the peptide linker of the CPD (CPD2). CPD2 was expressed in Escherichia coli, assembled into VLPs, purified and crystallized. A single crystal diffracted to 2.8 Å resolution and belonged to the cubic space group F432, with unit-cell parameters a = b = c = 218.6 Å. Single-crystal analysis showed that CPD1 and CPD2 rearranged into the same octahedral organization in a crystallization solution.

Keywords: enhanced green fluorescent protein; fusion protein; hepatitis B virus.

MeSH terms

  • Crystallization
  • Crystallography, X-Ray
  • Gene Expression Regulation, Viral*
  • Green Fluorescent Proteins / genetics*
  • Hepatitis B Core Antigens / chemistry
  • Hepatitis B Core Antigens / genetics*
  • Hepatitis B Core Antigens / metabolism
  • Hepatitis B virus / chemistry*
  • Hepatitis B virus / genetics
  • Hepatitis B virus / isolation & purification
  • Mutagenesis, Insertional* / genetics
  • Mutagenesis, Insertional* / immunology
  • Peptide Fragments / chemistry
  • Peptide Fragments / genetics*
  • Protein Multimerization* / physiology
  • Viral Core Proteins / chemistry*
  • Viral Core Proteins / genetics
  • Viral Core Proteins / isolation & purification

Substances

  • Hepatitis B Core Antigens
  • Peptide Fragments
  • Viral Core Proteins
  • enhanced green fluorescent protein
  • Green Fluorescent Proteins