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. 2013 Oct 25;52(44):11581-4.
doi: 10.1002/anie.201304579. Epub 2013 Sep 6.

Synthesis of Aryl Trimethylstannanes From Aryl Amines: A Sandmeyer-type Stannylation Reaction

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Synthesis of Aryl Trimethylstannanes From Aryl Amines: A Sandmeyer-type Stannylation Reaction

Di Qiu et al. Angew Chem Int Ed Engl. .

Abstract

Sandmeyer-type stannylation: Stille coupling is one of the most powerful coupling reactions for CC bond formation, whereas there are only limited methods to access aryl stannane compounds. A mild stannylation process based on a Sandmeyer-type transformation using aromatic amines as the starting materials is described. DCE: 1,2-dichloroethane.

Keywords: Sandmeyer reaction; Stille coupling reaction; aryl stannanes; cross-coupling; diazonium salts.

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