RISING beamline (BL28XU) for rechargeable battery analysis

J Synchrotron Radiat. 2014 Jan;21(Pt 1):268-72. doi: 10.1107/S1600577513025733. Epub 2013 Nov 28.

Abstract

The newly installed BL28XU beamline at SPring-8 is dedicated to in situ structural and electronic analysis of rechargeable batteries. It supports the time range (1 ms to 100 s) and spatial range (1 µm to 1 mm) needed for battery analysis. Electrochemical apparatus for battery charging and discharging are available in experimental hutches and in a preparation room. Battery analysis can be carried out efficiently and effectively using X-ray diffraction, X-ray absorption fine-structure analysis and hard X-ray photoelectron spectroscopy. Here, the design and performance of the beamline are described, and preliminary results are presented.

Keywords: X-ray absorption fine structure; in situ analysis; lithium-ion battery; time X-ray diffraction.