Solvent-dependent divergent functions of Sc(OTf)₃ in stereoselective epoxide-opening spiroketalizations

Org Lett. 2014 May 2;16(9):2474-7. doi: 10.1021/ol500853q. Epub 2014 Apr 17.

Abstract

A stereocontrolled synthesis of benzannulated spiroketals has been developed using solvent-dependent Sc(OTf)3-mediated spirocyclizations of exo-glycal epoxides having alcohol side chains. In THF, the reaction proceeds via Lewis acid catalysis under kinetic control with inversion of configuration at the anomeric carbon. In contrast, in CH2Cl2, Brønsted acid catalysis under thermodynamic control leads to retention of configuration. The reactions accommodate a variety of aryl substituents and ring sizes and provide stereochemically diverse spiroketals.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Epoxy Compounds / chemistry*
  • Furans / chemical synthesis*
  • Furans / chemistry
  • Lewis Acids / chemistry*
  • Mesylates / chemistry*
  • Molecular Structure
  • Scandium / chemistry*
  • Solvents / chemistry*
  • Spiro Compounds / chemical synthesis*
  • Spiro Compounds / chemistry
  • Stereoisomerism

Substances

  • Epoxy Compounds
  • Furans
  • Lewis Acids
  • Mesylates
  • Solvents
  • Spiro Compounds
  • scandium triflate
  • spiroketal
  • Scandium