EPSA: A Novel Supercritical Fluid Chromatography Technique Enabling the Design of Permeable Cyclic Peptides

ACS Med Chem Lett. 2014 Aug 4;5(10):1167-72. doi: 10.1021/ml500239m. eCollection 2014 Oct 9.

Abstract

Most peptides are generally insufficiently permeable to be used as oral drugs. Designing peptides with improved permeability without reliable permeability monitoring is a challenge. We have developed a supercritical fluid chromatography technique for peptides, termed EPSA, which is shown here to enable improved permeability design. Through assessing the exposed polarity of a peptide, this technique can be used as a permeability surrogate.

Keywords: EPSA; cyclic peptides; intramolecular hydrogen bonding; permeability; polarity.