Multispectroscopic DNA-binding studies of a terbium(III) complex containing 2,2'-bipyridine ligand

J Biomol Struct Dyn. 2016;34(2):414-26. doi: 10.1080/07391102.2015.1038585. Epub 2015 Jun 23.

Abstract

Agarose gel electrophoresis, absorption, fluorescence, viscosity, and circular dichroism (CD) have been used in exploring the interaction of terbium(III) complex, [Tb(bpy)2Cl3(OH2)] where bipy is 2,2'-bipyridine, with Fish salmon DNA. Agarose gel electrophoresis assay, along with absorption and fluorescence studies, reveal interaction between the corresponding complex and FS-DNA. Also, the binding constants (Kb) and the Stern-Volmer quenching constants (Ksv) of Tb(III) complex with FS-DNA were determined. The calculated thermodynamic parameters suggested that the binding of mentioned complex to FS-DNA was driven mainly by hydrophobic interactions. A comparative study of this complex with respect to the effect of iodide-induced quenching, ionic strength effect, and ethidium bromide exclusion assay reflects binding of explicit to the FS-DNA primarily in a groove fashion. CD and viscosity data also support the groove binding mode. Furthermore, Tb(III) complex have been simultaneously screened for their antibacterial and antifungal activities.

Keywords: 2,2′-bipyridine; DNA-binding; groove binding; spectroscopy; terbium(III) complex; thermodynamic parameters.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • 2,2'-Dipyridyl / pharmacology*
  • Absorption, Radiation
  • Animals
  • Anti-Infective Agents / pharmacology
  • Bacteria / drug effects
  • Binding Sites
  • Circular Dichroism
  • DNA / metabolism*
  • DNA Cleavage
  • Electrophoresis, Agar Gel
  • Ethidium / chemistry
  • Ethidium / metabolism
  • Fungi / drug effects
  • Kinetics
  • Ligands
  • Luminescence
  • Microbial Sensitivity Tests
  • Osmolar Concentration
  • Salmon
  • Spectrometry, Fluorescence
  • Temperature
  • Terbium / pharmacology*
  • Viscosity

Substances

  • Anti-Infective Agents
  • Ligands
  • Terbium
  • 2,2'-Dipyridyl
  • DNA
  • Ethidium