Effect of Different Surface Treatments on the Bond Strength of Lithium Disilicate Ceramic to the Zirconia Core

Photomed Laser Surg. 2016 Jun;34(6):236-43. doi: 10.1089/pho.2015.4063. Epub 2016 Apr 20.

Abstract

Objective: The aim of this study was to evaluate the effect of different surface treatments [sandblasting, Erbium:Yttrium-Aluminium-Garnet (Er:YAG), and femtosecond lasers] on the shear bond strength (SBS) of the CAD-on technique.

Background data: Although demand for all-ceramic restorations has increased, chipping remains one of the major problems for zirconia-based restorations.

Materials and methods: Forty yttrium-stabilized tetragonal zirconia polycrystalline (Y-TZP) zirconia plates (IPS e.max ZirCAD, Ivoclar Vivadent) were cut, sintered (12.4 × 11.4 × 3 mm) and divided into four groups according to the surface treatments (n = 10): a control group with no surface treatment (Group C), sandblasting with 50 μm Al2O3 (Group S), Er:YAG laser irradiation (Group E), and femtosecond laser irradiation (Group F). Also, 40 cylindrical (5 mm diameter, 2 mm height) lithium disilicate (IPS e.max CAD) veneer ceramics were cut and fused to all zirconia cores by a glass-fusion ceramic and crystallized according to the CAD-on technique. Specimens were subjected to shear force using a universal testing machine. The load was applied at a crosshead speed of 0.5 mm/min until failure. Mean SBS (MPa) were analyzed with one way ANOVA (p < 0.05). The failed specimens were examined under a stereomicroscope at ×20 to classify the mode of failure.

Results: The highest SBS was observed in Group F (36 ± 3.31 MPa), followed by Group S (33.03 ± 5.05 MPa), and Group C (32.52 ± 10.15 MPa). The lowest SBS was observed in Group E (31.02 ± 4.96 MPa), but no significant differences were found between the control and surface treated groups (p = 0.377). All the specimens showed a mixed type of failure.

Conclusions: Femtosecond laser application increased the bond strength between zirconia-veneer specimens. However, the novel CAD-on technique with no surface treatment also showed high bonding strength. Thus, this technique could prevent ceramic chipping without additional surface treatments.

MeSH terms

  • Air Abrasion, Dental
  • Ceramics / chemistry*
  • Dental Bonding*
  • Dental Porcelain / chemistry*
  • Dental Veneers
  • Humans
  • Lasers, Solid-State*
  • Materials Testing
  • Microscopy, Electron, Scanning
  • Shear Strength
  • Surface Properties
  • Zirconium / chemistry*

Substances

  • lithia disilicate
  • Dental Porcelain
  • Zirconium
  • zirconium oxide