Mutagenesis of mNeptune Red-Shifts Emission Spectrum to 681-685 nm

PLoS One. 2016 Apr 27;11(4):e0148749. doi: 10.1371/journal.pone.0148749. eCollection 2016.

Abstract

GFP-like fluorescent proteins with diverse emission wavelengths have been developed through mutagenesis, offering many possible choices in cellular and tissue imaging, such as multi-targets imaging, deep tissue imaging that require longer emission wavelength. Here, we utilized a combined approach of random mutation and structure-based rational design to develop new NIR fluorescent proteins on the basis of a far-red fluorescent protein, mNeptune (Ex/Em: 600/650 nm). We created a number of new monomeric NIR fluorescent proteins with the emission range of 681-685 nm, which exhibit the largest Stocks shifts (77-80 nm) compared to other fluorescent proteins. Among them, mNeptune681 and mNeptune684 exhibit more than 30 nm redshift in emission relative to mNeptune, owing to the major role of the extensive hydrogen-bond network around the chromophore and contributions of individual mutations to the observed redshift. Furthermore, the two variants still maintain monomeric state in solution, which is a trait crucial for their use as protein tags. In conclusion, our results suggest that there is untapped potential for developing fluorescent proteins with desired properties.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Green Fluorescent Proteins / genetics
  • Hydrogen Bonding
  • Luminescent Proteins / genetics*
  • Mutagenesis / genetics*
  • Mutation / genetics
  • Red Fluorescent Protein

Substances

  • Luminescent Proteins
  • Green Fluorescent Proteins

Grants and funding

This work was supported by the Chinese Academy of Sciences grant KJZD-EW-TZ-L04 to XEZ, and the National High Technology Research and Development Program ("863"Program) of China (No. 2011AA02A114, 2012AA022206) grant to DBW.