Molecular aspects of the interaction of spermidine and α-chymotrypsin

Int J Biol Macromol. 2016 Nov:92:523-532. doi: 10.1016/j.ijbiomac.2016.07.069. Epub 2016 Jul 22.

Abstract

Polyamines such as spermidine are essential for survival. The purpose of the present study was to investigate how spermidine could influence the conformation, thermal stability and the activity of α-chymotrypsin. The influence of spermidine on the structure and stability of α-Chymotrypsin (α-Chy) explored using different spectroscopy method and molecular docking simulations. The stability and activity of α-Chy were increased in the presence of spermidine. Increasing of the α-Chy absorption in the presence of spermidine was as a result of the formation of a spermidine - α-Chy complex. The results of fluorescence spectroscopic measurements suggested that spermidine has a vigorous ability to quench the intrinsic fluorescence of α-Chy through the dynamic quenching procedure. Near and Far-UV CD studies also confirmed the transfer of aromatic residues to a more flexible environment. The absorption increasing of α-Chy in the presence of spermidine was as a result of the formation of spermidine - α-Chy complex. Molecular docking results also revealed the presence of one binding site with a negative value for the Gibbs free energy of the binding of spermidine to α-Chy. Further, the docking study revealed that van der Waals interactions and hydrogen bonds play a main role in stabilizing the complex.

Keywords: Docking simulations; Dynamic quenching; Spectroscopic techniques; Thermal stability; α-Chymotrypsin.

MeSH terms

  • Chymotrypsin / metabolism*
  • Circular Dichroism
  • Enzyme Stability
  • Hydrogen Bonding
  • Hydrogen-Ion Concentration
  • Hydrophobic and Hydrophilic Interactions
  • Molecular Docking Simulation
  • Protein Binding
  • Protein Folding
  • Spectrometry, Fluorescence
  • Spectrophotometry, Ultraviolet
  • Spermidine / chemistry
  • Spermidine / metabolism*
  • Surface Properties
  • Transition Temperature

Substances

  • Chymotrypsin
  • alpha-chymotrypsin
  • Spermidine