Characterization of Wild Blueberry Polyphenols Bioavailability and Kinetic Profile in Plasma over 24-h Period in Human Subjects

Mol Nutr Food Res. 2017 Dec;61(12). doi: 10.1002/mnfr.201700405. Epub 2017 Nov 8.

Abstract

Scope: Understanding the metabolic fate of polyphenols from plant foods can aid in developing dietary recommendations that maximize their health benefits. Wild blueberries (WBB) provide a distinctive composition of dietary anthocyanins and chlorogenic acid (CGA).

Methods and results: This is a single blind, randomized, two-arm crossover controlled study. Human subjects ingested a WBB beverage (25 g freeze dried WBB powder) or placebo beverage with a meal and plasma was collected over 24 h. Anthocyanins, CGA and their metabolites were characterized and quantified in beverages and in plasma using targeted and non-targeted mass analyses. Bioavailability of WBB anthocyanins and 3-CGA was 1.1 and 0.2%, respectively. Parent anthocyanins and 3-CGA peaked ≈2 h post ingestion, while phase II metabolites, including glucuronide conjugates of peonidin, delphinidin, cyanidin and petunidin peaked ≈ 2.6, 6.3, 7 and 8.8 h, respectively. Phenolic acids (metabolites) peaked between 0.5 and 24 h. Biphasic responses were evident suggesting preferential enterohepatic recycling for some compounds.

Conclusion: The data indicate bioavailability of early and late phase WBB metabolites peaking at different times during the 24 h period, which may be important for maximizing their biological activity.

Trial registration: ClinicalTrials.gov NCT02167555.

Keywords: bioavailability; metabolites; pharmacokinetics; polyphenols; wild blueberry.

Publication types

  • Randomized Controlled Trial
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Adult
  • Anthocyanins / analysis
  • Biological Availability
  • Blueberry Plants / chemistry*
  • Chlorogenic Acid / analysis
  • Female
  • Fruit and Vegetable Juices / analysis
  • Humans
  • Hydroxybenzoates / blood
  • Hydroxybenzoates / pharmacokinetics
  • Male
  • Polyphenols / blood*
  • Polyphenols / pharmacokinetics*
  • Postprandial Period

Substances

  • Anthocyanins
  • Hydroxybenzoates
  • Polyphenols
  • Chlorogenic Acid
  • phenolic acid

Associated data

  • ClinicalTrials.gov/NCT02167555