Mapping Extracellular Matrix Proteins in Formalin-Fixed, Paraffin-Embedded Tissues by MALDI Imaging Mass Spectrometry

J Proteome Res. 2018 Jan 5;17(1):635-646. doi: 10.1021/acs.jproteome.7b00713. Epub 2017 Dec 11.

Abstract

Collagens and elastin form the fundamental framework of all tissues and organs, and their expression and post-translational processing are tightly regulated in disease and health. Because of their unique structural composition and properties, it is a recognized challenge to access these protein structures within the complex tissue microenvironment to understand how localized changes modulate tissue health. We describe a new workflow using a combination of matrix-assisted laser desorption/ionization imaging mass spectrometry (MALDI IMS) with matrix metalloproteinase (MMP) enzymes to access and report on spatial localization of collagen and elastin sequences in formalin-fixed, paraffin-embedded (FFPE) tissues. The developed technology provides new access to collagens and elastin sequences localized to tissue features that were previously unattainable. This high-throughput technological advance should be applicable to any tissue regardless of disease type, tissue origin, or disease status and is thus relevant to all research: basic, translational, or clinical.

Keywords: MALDI imaging mass spectrometry; extracellular matrix; formalin-fixed, paraffin-embedded tissue imaging; imaging mass spectrometry; peptide imaging; proteomics; tissue imaging.

Publication types

  • Research Support, N.I.H., Extramural
  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Collagen / analysis
  • Elastin / analysis
  • Extracellular Matrix Proteins / analysis*
  • Formaldehyde
  • Humans
  • Matrix Metalloproteinases
  • Paraffin Embedding
  • Spectrometry, Mass, Matrix-Assisted Laser Desorption-Ionization / methods*
  • Tissue Fixation

Substances

  • Extracellular Matrix Proteins
  • Formaldehyde
  • Collagen
  • Elastin
  • Matrix Metalloproteinases