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. 2018 Jan 19;20(2):465-468.
doi: 10.1021/acs.orglett.7b03846. Epub 2018 Jan 9.

Synthesis of Unsymmetric Trisulfides From 9-Fluorenylmethyl Disulfides

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Free PMC article

Synthesis of Unsymmetric Trisulfides From 9-Fluorenylmethyl Disulfides

Shi Xu et al. Org Lett. .
Free PMC article

Abstract

A convenient method for the preparation of unsymmetrical trisulfides using 9-fluorenylmethyl (Fm) disulfide as the precursors is reported. This method gives the desired trisulfides in good yields under mild conditions.

Conflict of interest statement

The authors declare no competing financial interest.

Figures

Figure 1
Figure 1
Representative trisulfide molecules.
Scheme 1
Scheme 1
Synthetic Methods for Trisulfides
Scheme 2
Scheme 2
Proposed Mechanism for the Generation of 6
Scheme 3
Scheme 3
Proposed Mechanism for Disulfide Formation

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