Sufficiency of curing in high-viscosity bulk-fill resin composites with enhanced opacity

Clin Oral Investig. 2019 Feb;23(2):747-755. doi: 10.1007/s00784-018-2482-2. Epub 2018 May 18.

Abstract

Objectives: The study aims analyzing if improved opacity in modern high-viscosity bulk-fill resin composites (BF-RBC) contradicts with the sufficiency of curing and to assess material's tolerance to less ideal curing conditions.

Materials and methods: Simulated large cavities (10 × 6) mm were filled in one increment with three BF-RBCs (Filtek One, FO; Tetric Evo Ceram Bulk Fill, TEC-BF; SonicFill2, SF2). One central and two peripheral (4 mm apart from the center) micromechanical property line-profiles (HV, Vickers hardness; YHU, indentation modulus) were measured in 0.2-mm steps at 24 h post-polymerization (n = 6). Depth of cure (DOC) was calculated from the HV variation in depth. A scratch test (DOCscratch test) estimated the tolerance in polymerization when simulating clinically relevant curing conditions (exposure distance up to 7 mm; centered and with a 3-mm offset placement of the LCU). Irradiance and spectral distribution of the used light curing unit (LCU) were assessed at various curing conditions.

Results: DOC varied among 3.6 mm (SF2, peripheral) and 5.7 mm (FO, central). The BF-RBC influences DOC stronger (p < 0.001, ηP2 = 0.616) than the width (p < 0.001, ηP2 = 0.398). Significant lower DOC (t test) was measured peripheral compared to center in all materials. YHU was more sensitive to the varied parameters as HV. DOCscratch test varied among 2.4 mm (SF2, 3-mm offset, exposure distance 7 mm) and 3.9 mm (FO, center, 0 mm).

Conclusions: Whether opacity competes with DOC is material dependent. BF-RBCs tolerate small variations in LCU's centricity better than variations in exposure distance.

Clinical relevance: The upper incremental thickness threshold of 4 or 5 mm was not reached in all BF-RBCs under simulated clinically relevant curing conditions.

Keywords: Bulk-fill resin composite; Depth of cure; Hardness; Indentation modulus; LCU; Opacity; Translucency.

MeSH terms

  • Composite Resins / chemistry*
  • Dental Materials / chemistry*
  • Elastic Modulus
  • Hardness
  • Light-Curing of Dental Adhesives*
  • Materials Testing
  • Polymerization
  • Surface Properties
  • Viscosity

Substances

  • Composite Resins
  • Dental Materials