The repair bond strength to resin matrix in cured resin composites after water aging

Dent Mater J. 2019 Mar 31;38(2):233-240. doi: 10.4012/dmj.2018-044. Epub 2018 Nov 17.

Abstract

The repair microshear bond strengths (µSBSs) to resin matrices in 4 different cured-composites after water storage (0, 60 s, 1 week, 1 month) were evaluated. Three different adhesive application methods to the cured-composites were performed; (1) none, (2) onestep self-etch adhesive application, and (3) one-step self-etch adhesive application with a silane coupling agent. Degree of conversion (DC) of the composite discs was determined using ATR/FT-IR with a time-based spectrum analysis. Initially, the amount of un-reacted resin monomers in the repaired cured-composite contributed to the bonding performance of newly-filled uncured-composite to resin matrix of the cured-composite. Adhesive application could not improve their repair µSBS. After 1-month of water-storage, the repair µSBS was dependent on material, which either reduced or did not and was not influenced by their amount of un-reacted resin monomers. When repairing aged composite resin, the appropriate adhesive application procedures were different among resin composites.

Keywords: Adhesive application; Degree of conversion; Repair bond strength; Resin matrix; Water aging.

MeSH terms

  • Composite Resins
  • Dental Bonding*
  • Materials Testing
  • Resin Cements*
  • Spectroscopy, Fourier Transform Infrared
  • Surface Properties
  • Tensile Strength
  • Water

Substances

  • Composite Resins
  • Resin Cements
  • Water