Structure elaboration of isoniazid: synthesis, in silico molecular docking and antimycobacterial activity of isoniazid-pyrimidine conjugates

Mol Divers. 2020 Nov;24(4):949-955. doi: 10.1007/s11030-019-10004-1. Epub 2019 Oct 18.

Abstract

Designing small molecule-based new drug candidates through structure modulation of the existing drugs has drawn considerable attention in view of inevitable emergence of resistance. A new series of isoniazid-pyrimidine conjugates were synthesized in good yields and evaluated for antitubercular activity against the H37Rv strain of Mycobacterium tuberculosis using the microplate Alamar Blue assay. Structure-anti-TB relationship profile revealed that conjugates 8a and 8c bearing a phenyl group at C-6 of pyrimidine scaffold were most active (MIC99 10 µM) and least cytotoxic members of the series. In silico docking of 8a in the active site of bovine lactoperoxidase as well as a cytochrome C peroxidase mutant N184R Y36A revealed favorable interactions similar to the heme enzyme catalase peroxidase (KatG) that activates isoniazid. This investigation suggests a rationale for further work on this promising series of antitubercular agents.

Keywords: ADME; Conjugates; Drug resistance; Isoniazid; Molecular docking; Pyrimidine; Tuberculosis.

MeSH terms

  • Animals
  • Antitubercular Agents / chemical synthesis*
  • Antitubercular Agents / chemistry*
  • Antitubercular Agents / pharmacology
  • Catalytic Domain / drug effects
  • Cattle
  • Cytochrome-c Peroxidase / metabolism
  • Isoniazid / chemical synthesis*
  • Isoniazid / chemistry*
  • Lactoperoxidase / metabolism
  • Molecular Docking Simulation / methods
  • Mycobacterium tuberculosis / drug effects
  • Peroxidase / metabolism
  • Pyrimidines / chemical synthesis*
  • Pyrimidines / chemistry*
  • Small Molecule Libraries / chemical synthesis
  • Small Molecule Libraries / chemistry
  • Small Molecule Libraries / pharmacology

Substances

  • Antitubercular Agents
  • Pyrimidines
  • Small Molecule Libraries
  • Lactoperoxidase
  • Cytochrome-c Peroxidase
  • Peroxidase
  • Isoniazid