High-throughput, Multi-batch System for the Efficient Microwave Digestion of Biological Samples

Anal Sci. 2020 Jul 10;36(7):889-892. doi: 10.2116/analsci.19A004. Epub 2020 Jan 31.

Abstract

In this paper, we proposed a high-throughput microwave digestion system based on multi-batch reactors (three quartz test tubes inside commercial PTFE vessels). This original configuration was validated by ICP-MS analysis of several elements in biological certified reference materials (fish tissues and plankton). The proposed system was proved to be free from contamination showing very low LODs. The improved hardware configuration is therefore highly beneficial for the detection of trace elements in microsamples from the marine food web.

Keywords: High-throughput microwave digestion; biological samples; marine food web; microsamples; trace elements.

MeSH terms

  • Animals
  • Fishes
  • High-Throughput Screening Assays*
  • Mass Spectrometry
  • Microwaves*
  • Plankton
  • Trace Elements / analysis*
  • Trace Elements / metabolism

Substances

  • Trace Elements