Cryo-EM structures reveal intricate Fe-S cluster arrangement and charging in Rhodobacter capsulatus formate dehydrogenase

Nat Commun. 2020 Apr 20;11(1):1912. doi: 10.1038/s41467-020-15614-0.

Abstract

Metal-containing formate dehydrogenases (FDH) catalyse the reversible oxidation of formate to carbon dioxide at their molybdenum or tungsten active site. They display a diverse subunit and cofactor composition, but structural information on these enzymes is limited. Here we report the cryo-electron microscopic structures of the soluble Rhodobacter capsulatus FDH (RcFDH) as isolated and in the presence of reduced nicotinamide adenine dinucleotide (NADH). RcFDH assembles into a 360 kDa dimer of heterotetramers revealing a putative interconnection of electron pathway chains. In the presence of NADH, the RcFDH structure shows charging of cofactors, indicative of an increased electron load.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Carbon Dioxide / metabolism
  • Catalysis
  • Catalytic Domain
  • Cryoelectron Microscopy / methods*
  • Formate Dehydrogenases / chemistry*
  • Models, Molecular
  • Molybdenum / chemistry
  • NAD / chemistry
  • NAD / metabolism
  • Oxidation-Reduction
  • Rhodobacter capsulatus / metabolism*
  • Tungsten

Substances

  • NAD
  • Carbon Dioxide
  • Molybdenum
  • Formate Dehydrogenases
  • Tungsten