Deleterious effect of Brij 35 on alkyl 2-pyrones and other hydrophobic inhibitors of human sputum and leucocyte elastase

Biochem Int. 1988 Oct;17(4):637-46.

Abstract

Brij 35 significantly reduced the inhibitory activity of hydrophobic alkyl 2-pyrones, oleic acid and alkyl peptides towards human sputum and leucocyte elastase, whereas 4-methoxy-6-(2'-hydroxy-2'-(carbobutyloxy)-vinyl)-2-pyrone, alpha-1-proteinase inhibitor and a sulfated chitosan were unaffected. The effect of Brij 35 on elastase appeared to be irreversible, since dialysis against Brij-free buffer was not accompanied by a return to inhibitory activity by the first group of inhibitors. However, passage through an ionic-exchange column was effective in removing the detergent from the enzyme. Brij 35 is also an activator of the elastases: kcat for Boc-Ala-4-nitrophenyl ester and methylsuccinyl-Ala-Ala-Pro-Val-4-nitroanilide increased by 20% and 40%, respectively in the presence of 0.015% Brij 35. Binding of the substrates to the enzyme is unaffected, since Km is unchanged.

MeSH terms

  • Detergents / adverse effects*
  • Electrophoresis, Polyacrylamide Gel
  • Enzyme Activation
  • Humans
  • Hydrolysis
  • Kinetics
  • Pancreatic Elastase / antagonists & inhibitors*
  • Polidocanol
  • Polyethylene Glycols / adverse effects*
  • Surface-Active Agents / adverse effects*

Substances

  • Detergents
  • Surface-Active Agents
  • Polidocanol
  • Polyethylene Glycols
  • Pancreatic Elastase