High-Throughput Analyses of Microplastic Samples Using Fourier Transform Infrared and Raman Spectrometry

Appl Spectrosc. 2020 Sep;74(9):1185-1197. doi: 10.1177/0003702820932926. Epub 2020 Jun 19.

Abstract

Determining microplastics in environmental samples quickly and reliably is a challenging task. With a largely automated combination of optical particle analysis, Fourier transform infrared (FT-IR), and Raman microscopy along with spectral database search, particle sizes, particle size distributions, and the type of polymer including particle color can be determined. We present a self-developed, open-source software package for realizing a particle analysis approach with both Raman and FT-IR microspectroscopy. Our software GEPARD (Gepard Enabled PARticle Detection) allows for acquiring an optical image, then detects particles and uses this information to steer the spectroscopic measurement. This ultimately results in a multitude of possibilities for efficiently reviewing, correcting, and reporting all obtained results.

Keywords: FT-IR; Fourier transform infrared; Microplastics; Open Source; Raman; microspectroscopy.

MeSH terms

  • Environmental Monitoring / methods*
  • Environmental Pollutants / analysis*
  • High-Throughput Screening Assays
  • Microplastics / analysis*
  • Software*
  • Spectroscopy, Fourier Transform Infrared
  • Spectrum Analysis, Raman

Substances

  • Environmental Pollutants
  • Microplastics