The Effects of Silver, Zinc Oxide, and Titanium Dioxide Nanoparticles Used as Dentin Pretreatments on the Microshear Bond Strength of a Conventional Glass Ionomer Cement to Dentin

Int J Nanomedicine. 2020 Jul 6:15:4755-4762. doi: 10.2147/IJN.S262664. eCollection 2020.

Abstract

Aim: This study was conducted to evaluate the effects of three nanoparticle solutions used as dentin pretreatments on the microshear bond strength (µSBS) of a conventional glass ionomer cement (GIC) to dentin.

Materials and methods: Ninety intact human molars were used after sectioning their occlusal surfaces to expose flat dentin surfaces. The specimens were randomly assigned to nine groups (n = 10). Group A was the control group (without using the cavity disinfectant). In groups B, C, D, and E, the prepared dentin surfaces were treated with 1 cc 2% chlorhexidine (CHX), 0.1% silver nanoparticle (SNP), 0.1% titanium dioxide nanoparticle (TNP), and 0.1% zinc oxide nanoparticle (ZNP) solutions for 1 minute, respectively, before applying the conditioner. CHX, SNPs, TNPs, and ZNPs were applied for 1 minute after applying the conditioner in groups F, G, H, and I, respectively. The specimens were restored with a conventional GIC and underwent µSBS testing after 24 hours. The data were analyzed using the one-way analysis of variance and Tukey's test (p=0.05).

Results: The applications of the nanoparticles (SNP, TNP, and ZNP) after the conditioner were associated with significantly greater µSBS values compared to that of the control group (p values < 0.05). Significantly higher µSBS values were observed when TNP or ZNP was applied after the conditioner compared to their applications before the conditioner (p values < 0.05). The highest µSBS values were observed when TNP was applied after the conditioner.

Conclusion: Dentin pretreatment with the nanoparticles after applying the conditioner enhanced the bond strength of the GIC to dentin compared with the control group. The best results were obtained for the TNPs applied after the conditioner.

Keywords: glass ionomer cement; microshear bond strength; nanoparticles.

MeSH terms

  • Chlorhexidine / pharmacology
  • Dental Bonding*
  • Dentin / drug effects*
  • Glass Ionomer Cements / chemistry
  • Glass Ionomer Cements / pharmacology*
  • Humans
  • Materials Testing
  • Metal Nanoparticles / chemistry*
  • Silver / pharmacology*
  • Surface Properties
  • Titanium / pharmacology*
  • Zinc Oxide / pharmacology*

Substances

  • Glass Ionomer Cements
  • titanium dioxide
  • Silver
  • Titanium
  • Chlorhexidine
  • Zinc Oxide