Kinomic profile in patient-derived glioma cells during hypoxia reveals c-MET-PI3K dependency for adaptation

Theranostics. 2021 Mar 5;11(11):5127-5142. doi: 10.7150/thno.54741. eCollection 2021.

Abstract

Hypoxic microenvironment is a hallmark of solid tumors, especially glioblastoma. The strong reliance of glioma-propagating cells (GPCs) on hypoxia-induced survival advantages is potentially exploitable for drug development. Methods: To identify key signaling pathways for hypoxia adaptation by patient-derived GPCs, we performed a kinase inhibitor profiling by screening 188 small molecule inhibitors against 130 different kinases in normoxia and hypoxia. Potential kinase candidates were prioritized for in vitro and in vivo investigations using a ranking algorithm that integrated information from the kinome connectivity network and estimated patients' survival based on expression status. Results: Hypoxic drug screen highlighted extensive modifications of kinomic landscape and a crucial functionality of c-MET-PI3K. c-MET inhibitors diminished phosphorylation of c-MET and PI3K in GPCs subjected to hypoxia, suggesting its role in the hypoxic adaptation of GPCs. Mechanistically, the inhibition of c-MET and PI3K impaired antioxidant defense, leading to oxidative catastrophe and apoptosis. Repurposed c-MET inhibitors PF04217903 and tivantinib exhibited hypoxic-dependent drug synergism with temozolomide, resulting in reduced tumor load and growth of GPC xenografts. Detailed analysis of bulk and single-cell glioblastoma transcriptomes associates the cellular subpopulation over-expressing c-MET with inflamed, hypoxic, metastatic, and stem-like phenotypes. Conclusions: Thus, our "bench to bedside (the use of patient-derived GPCs and xenografts for basic research) and back (validation with independent glioblastoma transcriptome databases)" analysis unravels the novel therapeutic indications of c-MET and PI3K/Akt inhibitors for the treatment of glioblastoma, and potentially other cancers, in the hypoxic tumor microenvironment.

Keywords: HIF-1α; PI3K; glioblastoma; oxidative stress; tumor microenvironment.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Animals
  • Antioxidants / pharmacology
  • Apoptosis / drug effects
  • Apoptosis / genetics
  • Brain Neoplasms / drug therapy
  • Brain Neoplasms / genetics
  • Cell Line, Tumor
  • Glioblastoma / drug therapy
  • Glioblastoma / genetics
  • Glioma / drug therapy
  • Glioma / genetics*
  • Humans
  • Hypoxia / drug therapy
  • Hypoxia / genetics*
  • Male
  • Mice
  • Phosphatidylinositol 3-Kinases / genetics*
  • Phosphorylation / drug effects
  • Phosphorylation / genetics
  • Proto-Oncogene Proteins c-met / genetics*
  • Pyrazines / pharmacology
  • Pyrrolidinones / pharmacology
  • Quinolines / pharmacology
  • Signal Transduction / drug effects
  • Signal Transduction / genetics
  • Temozolomide / pharmacology
  • Transcriptome / drug effects
  • Transcriptome / genetics
  • Triazoles / pharmacology

Substances

  • 2-(4-(3-quinolin-6-ylmethyl-3H-(1,2,3)triazolo(4,5-b)pyrazin-5-yl)pyrazol-1-yl)ethanol
  • ARQ 197
  • Antioxidants
  • Pyrazines
  • Pyrrolidinones
  • Quinolines
  • Triazoles
  • MET protein, human
  • Proto-Oncogene Proteins c-met
  • Temozolomide