Measurement of Plasma Glucagon Levels Using Mass Spectrometry in Patients with Type 2 Diabetes on Maintenance Hemodialysis

Kidney Blood Press Res. 2021;46(5):652-656. doi: 10.1159/000518027. Epub 2021 Aug 17.

Abstract

Background: Recently, attention has been focused on the effect of glucagon on blood glucose variability. The dynamics of glucagon have attracted attention as a new target in the treatment of diabetes patients. However, the dynamics of glucagon in hemodialysis (HD) patients with type 2 diabetes mellitus (T2DM) remain unclear.

Objectives: The aim of this study was to assess the dynamics of glucagon in HD patients with T2DM.

Materials and methods: We measured plasma glucagon in HD patients with T2DM by liquid chromatography-high-resolution mass spectrometry (LC-HRMS), sandwich enzyme-linked immunosorbent assay (ELISA), and radioimmunoassay (RIA). The glucagon levels measured by each method were compared. We used the glucagon levels determined by our developed LC-HRMS method as the standard in this study.

Results: Plasma glucagon levels measured by LC-HRMS before HD were significantly higher than those measured after HD. Plasma glucagon levels measured using sandwich ELISA had a significantly higher correlation with those measured using LC-HRMS compared with RIA.

Conclusions: This was the first study to assess glucagon levels in HD patients with T2DM using LC-HRMS, which is considered a highly accurate method. Sandwich ELISA was shown to measure glucagon levels accurately as well.

Keywords: Hemodialysis; Liquid chromatography-high-resolution mass spectrometry; Plasma glucagon.

MeSH terms

  • Aged
  • Chromatography, Liquid
  • Diabetes Mellitus, Type 2 / blood*
  • Female
  • Glucagon / blood*
  • Humans
  • Male
  • Mass Spectrometry
  • Middle Aged
  • Renal Dialysis*

Substances

  • Glucagon