Preparation, Characterization, and Electrochemical Performance of the Hematite/Oxidized Multi-Walled Carbon Nanotubes Nanocomposite

Molecules. 2022 Apr 22;27(9):2708. doi: 10.3390/molecules27092708.

Abstract

In this research work, a hematite (α-Fe2O3) nanoparticle was prepared and then mixed with oxidized multi-walled carbon nanotubes (O-MWCNT) to form a stable suspension of an α-Fe2O3/O-MWCNTs nanocomposite. Different characterization techniques were used to explore the chemical and physical properties of the α-Fe2O3/O-MWCNTs nanocomposite, including XRD, FT-IR, UV-Vis, and SEM. The results revealed the successful formation of the α-Fe2O3 nanoparticles, and the oxidation of the MWCNT, as well as the formation of stable α-Fe2O3/O-MWCNTs nanocomposite. The electrochemical behaviour of the α-Fe2O3/O-MWCNTs nanocomposite was investigated using cyclic voltammetry (CV) and linear sweep voltammetry (LSV), and the results revealed that modification of α-Fe2O3 nanoparticles with O-MWCNTs greatly enhanced electrochemical performance and capacitive behaviour, as well as cycling stability.

Keywords: MWCNT; capacitive behaviour; electrochemical performance; hematite; nanoparticle.

MeSH terms

  • Electrochemical Techniques / methods
  • Ferric Compounds
  • Nanocomposites* / chemistry
  • Nanotubes, Carbon* / chemistry
  • Spectroscopy, Fourier Transform Infrared

Substances

  • Ferric Compounds
  • Nanotubes, Carbon
  • ferric oxide