Primer application technique and remaining dentin thickness affected microtensile bond strength of contemporary dentin adhesives under simulated pulp pressure

Clin Oral Investig. 2023 Jan;27(1):139-149. doi: 10.1007/s00784-022-04699-0. Epub 2022 Sep 16.

Abstract

Objectives: To evaluate the effect of application techniques, type of adhesives and remaining dentin thicknesses on microtensile bond strength (µTBS) of 3 adhesive systems.

Materials and methods: 112 flat occlusal dentinal surfaces of third molar were randomly allocated into 16 groups based on 2 remaining dentin thicknesses (RDT), 2 application techniques, and 3 adhesive systems (Optibond FL, OFL; Clearfil SE Bond, CSE; and Single Bond Universal, SB); SB was applied in either etch-and-rinse (ER) or self-etch (SE) mode. Simulated pulpal pressure was performed during restorative procedure and water storage. The stick-shaped specimens from each tooth underwent µTBS testing. The data were evaluated using a paired t test and ANOVA followed by a post hoc test. The fractured specimens were evaluated for mode of failure using a stereomicroscope.

Results: The mean µTBS values were significantly affected by RDT, application technique, and types of adhesives. Neither RDT nor application technique affected µTBS of SB in ER mode, whereas application technique affected both conventional and universal self-etch adhesives. RDT also influenced µTBS of OFL.

Conclusions: RDT and application technique differently affected the µTBS of dentin bonding which was product-related. Etch-and-rinse systems had higher bond strength to superficial than to deep dentin, whereas self-etch systems were more sensitive to both RDT and application technique.

Clinical relevance: The universal adhesive is less sensitive to intrinsic wetness and can be used according to manufacturer's instructions.

Keywords: Microtensile bond strength; Primer application technique; Remaining dentin thickness; Simulated pulp pressure.

MeSH terms

  • Adhesives
  • Dental Bonding*
  • Dental Cements*
  • Dentin
  • Dentin-Bonding Agents / chemistry
  • Materials Testing
  • Resin Cements / chemistry
  • Tensile Strength

Substances

  • Dental Cements
  • Dentin-Bonding Agents
  • Resin Cements
  • Adhesives