Effect of different surface treatment protocols on the bond strength between lithium disilicate and resin cements

Odontology. 2024 Jan;112(1):74-82. doi: 10.1007/s10266-023-00809-w. Epub 2023 Apr 10.

Abstract

Because the use of hydrofluoric acid (HF) poses health risks if handled improperly, many clinicians prefer to have the ceramic restorations pre-etched in dental laboratories. However, during the try-in procedure, the pre-etched glass-ceramic restorations may be contaminated with saliva resulting in reduced bond strength. This in-vitro study aimed to investigate the effect of different surface treatments on the bond strength of lithium disilicate (LD) glass-ceramic restorations (IPS e.max Press, Ivoclar Vivadent) to two resin cements. One-hundred eighty blocks (4X4X3mm) of LD glass-ceramic were divided into twelve groups (n = 15), of which six received Variolink Esthetic DC (VE) cement and six received RelyX Ultimate (RU) cement, following the surface treatments: G1) Control: Hydrofluoric Acid + Silane (HF + Sil); G2) Hydrofluoric Acid + Saliva + Silane (HF + S + Sil); G3) Hydrofluoric Acid + Saliva + Ivoclean + Silane (HF + S + IC + Sil); G4) Hydrofluoric Acid + Saliva + Phosphoric Acid + Silane (HF + S + P + Sil); G5) Hydrofluoric Acid + Saliva + Monobond Etch & Prime (HF + S + EP); G6) Monobond Etch & Prime (EP). Following treatment, a resin-cement cylinder (2.3 mm diameter) was built on the glass-ceramic surface, photocured (20 s), stored in distilled water (37 °C, 24 h) and submitted to the shear bond strength test. Bond strength data (MPa) were subjected to two-way ANOVA and Tukey (α = 0.01). Cement type and surface treatment had a significant effect on the bond strength (p < 0.001) (Table 4). Single-step Monobond Etch & Prime (EP) significantly improved the bond strength of resin-cements to glass-ceramic with and without saliva contamination.

Keywords: Bond strength; Ceramic; Lithium disilicate; Resin cement; Surface treatment.

MeSH terms

  • Ceramics
  • Clinical Protocols
  • Dental Bonding*
  • Dental Cements
  • Dental Porcelain
  • Diphosphates
  • Ethanol
  • Hydrofluoric Acid
  • Materials Testing
  • Methacrylates
  • Resin Cements* / chemistry
  • Silanes
  • Surface Properties

Substances

  • Resin Cements
  • Hydrofluoric Acid
  • Silanes
  • Dental Porcelain
  • Dental Cements
  • lithia disilicate
  • Etch&Prime
  • Ethanol
  • Methacrylates
  • Diphosphates