Effect of different surface roughening treatment on polyether ether ketone and acrylic resin bonding: A pilot study

Dent Med Probl. 2024 Mar-Apr;61(2):249-255. doi: 10.17219/dmp/133071.

Abstract

Background: As polyether ether ketone (PEEK) is a relatively new material in dentistry, its bonding properties with regard to dental acrylic base materials are not fully known. To ensure the long-term success of removable dentures with a PEEK framework, the base materials must be well bonded to each other.

Objectives: The study aimed to investigate the effects of different kinds of surface roughening treatment on PEEK and acrylic resin bonding.

Material and methods: Eighty PEEK specimens (N = 80) were randomly divided into 5 groups (n = 16 per group) and subjected to various surface roughening treatment (control, grinding, sandblasting, tribochemical silica coating (CoJet), and sulfuric acid etching). Heat-polymerized acrylic resin was applied to the treated surfaces of the PEEK specimens. The shear bond strength (SBS) test, environmental scanning electron microscopy (ESEM) analysis and three-dimensional (3D) surface topography analysis were performed. The statistical analysis of the data was conducted using the analysis of variance (ANOVA) and Tukey's multiple comparison test.

Results: The one-way ANOVA showed significant differences in the SBS values between the groups (p = 0.001). Sandblasting, tribochemical silica coating and sulfuric acid etching resulted in high SBS values (p = 0.001). The highest SBS values were observed in the sulfuric acid etching group (8.83 ±3.63 MPa), while the lowest SBS values were observed in the control group (3.33 ±2.50 MPa).

Conclusions: The additional roughening treatment applied to the PEEK surface increases the bond strength with heat-polymerized acrylic resin.

Keywords: CoJet; polyether ether ketone; sandblasting; sulfuric acid; surface morphology.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Acrylic Resins* / chemistry
  • Benzophenones*
  • Dental Bonding*
  • Dental Stress Analysis
  • Humans
  • Ketones* / chemistry
  • Materials Testing
  • Microscopy, Electron, Scanning
  • Pilot Projects
  • Polyethylene Glycols* / chemistry
  • Polymers*
  • Shear Strength
  • Sulfuric Acids / chemistry
  • Surface Properties*

Substances

  • polyetheretherketone
  • Ketones
  • Benzophenones
  • Polymers
  • Polyethylene Glycols
  • Acrylic Resins
  • Sulfuric Acids
  • sulfuric acid