Assembly of a multivalent aptamer for efficient inhibition of thermostable direct hemolysin toxicity induced by Vibrio parahaemolyticus

J Hazard Mater. 2024 Oct 5:478:135452. doi: 10.1016/j.jhazmat.2024.135452. Epub 2024 Aug 6.

Abstract

Thermostable direct hemolysin (TDH) is a key virulence factor of Vibrio parahaemolyticus, capable of causing seafood-mediated outbreaks of gastroenteritis, posing a threat to the aquatic environment and global public health. In the present study, we explored a multivalent aptamer-mediated inhibition strategy to mitigate TDH toxicity. Based on the characteristic structure of TDH, a stable multivalent aptamer, Ap3-5, was rationally designed by truncation, key fragment evolution, and end fixation. Ap3-5 exhibited strong affinity (Kd=39.24 nM), and thermal (Tm=57.6 °C) and enzymatic stability. In silico studies also revealed that Ap3-5 occupied more active sites of TDH and covered its central pore, indicating its potential as a blocking agent for inhibiting TDH toxicity. In the hemolysis assay, Ap3-5 significantly suppressed the hemolytic effect of TDH. A cellular study revealed a substantial (∼80 %) reduction in TDH cytotoxicity. Supporting these findings, in vivo trials confirmed the inhibitory action of Ap3-5 on both the acute and intestinal toxicity of TDH. Overall, benefiting from the strong binding affinity, high stability, and multisite occupation of the multivalent aptamer with TDH, Ap3-5 displayed robust potential against TDH toxicity by inhibiting membrane pore formation, providing a new approach for alleviating bacterial infections.

Keywords: Molecular docking; Multivalent aptamer; TDH; Toxicity inhibition.

MeSH terms

  • Animals
  • Aptamers, Nucleotide* / chemistry
  • Bacterial Proteins / genetics
  • Bacterial Proteins / metabolism
  • Bacterial Proteins / toxicity
  • Bacterial Toxins* / chemistry
  • Bacterial Toxins* / toxicity
  • Hemolysin Proteins* / chemistry
  • Hemolysin Proteins* / toxicity
  • Hemolysis* / drug effects
  • Humans
  • Vibrio parahaemolyticus* / drug effects
  • Vibrio parahaemolyticus* / genetics

Substances

  • Hemolysin Proteins
  • thermostable direct hemolysin
  • Aptamers, Nucleotide
  • Bacterial Toxins
  • Bacterial Proteins