High-performance removal of methylene blue dye using porous lignin extracted from sugarcane bagasse by deep eutectic solvent

Int J Biol Macromol. 2024 Nov;279(Pt 3):135470. doi: 10.1016/j.ijbiomac.2024.135470. Epub 2024 Sep 7.

Abstract

This study evaluated the ability of triethyl benzyl ammonium chloride/lactic acid deep eutectic solvent extracted lignin (TEBAC/LA-DES-L) to adsorb methylene blue (MB) without additional functional group modification. The structure and morphology of TEBAC/LA-DES-L were characterized using SEM, BET, FT-IR, and TGA techniques. Various factors influencing MB adsorption, such as extraction temperature, solution pH, adsorbent dose, initial MB concentration, adsorption time, and reaction temperature, were investigated. The Redlich-Peterson isotherm displayed a good fit for the experimental data, with a maximum adsorption capacity of 85.16 mg/g. Kinetic analysis suggested that the adsorption process followed the pseudo-second-order model, with adsorption occurring in <100 min on DES-L-4 h. The mechanism of MB adsorption on DES-L-4 h was attributed to electrostatic attraction, hydrophobic interactions, and hydrogen bonding forces. Overall, DES-L-4 h demonstrated high adsorption capacity and rapid adsorption rate, making it a promising adsorbent for effectively removing cationic dyes from wastewater.

Keywords: Adsorption; Deep eutectic solvent; Isotherm; Lignin; Methylene blue.

MeSH terms

  • Adsorption
  • Cellulose* / chemistry
  • Coloring Agents / chemistry
  • Coloring Agents / isolation & purification
  • Deep Eutectic Solvents* / chemistry
  • Hydrogen-Ion Concentration
  • Kinetics
  • Lignin* / chemistry
  • Methylene Blue* / chemistry
  • Methylene Blue* / isolation & purification
  • Porosity
  • Saccharum* / chemistry
  • Temperature
  • Wastewater / chemistry
  • Water Pollutants, Chemical* / chemistry
  • Water Pollutants, Chemical* / isolation & purification
  • Water Purification / methods

Substances

  • Methylene Blue
  • Lignin
  • Cellulose
  • Water Pollutants, Chemical
  • Deep Eutectic Solvents
  • bagasse
  • Coloring Agents
  • Wastewater