Phenylboronic Acid-Modified Polyethyleneimine: A Glycan-Targeting Anti-Biofilm Polymer for Inhibiting Bacterial Adhesion to Mucin and Enhancing Antibiotic Efficacy

ACS Appl Mater Interfaces. 2025 Apr 2;17(13):19276-19285. doi: 10.1021/acsami.4c20874. Epub 2025 Mar 18.

Abstract

Bacterial biofilms present significant therapeutic challenges due to their resistance to conventional antimicrobial treatment. Mucins typically serve as a protective barrier against pathogens, yet certain bacteria, such as Pseudomonas aeruginosa (P. aeruginosa), can exploit these glycoproteins as attachment sites for biofilm formation. This study introduces boronic acid-functionalized polyethyleneimine (PEI-BA) as a promising antibiofilm agent that effectively blocks bacterial adhesion to mucin-rich surfaces. Through the multivalent presentation of boronic acid groups, PEI-BA reversibly forms boronate ester bonds with mucin glycans, creating a protective barrier. Our findings show that PEI-BA prevents bacterial attachment through a nonbactericidal mechanism, potentially reducing the risk of resistance development. Notably, PEI-BA synergizes with a conventional antibiotic, tobramycin, significantly enhancing biofilm inhibition compared to either treatment alone. Systematic evaluation of PEI-BA formulations identified optimal functionalization levels, balancing glycan-binding capability with solubility. From a biomaterials design perspective, we demonstrate how rational polymer modification can transform a potent but cytotoxic antimicrobial agent (i.e., PEI) into a safe and effective antibiofilm material, opening further possibilities for managing biofilm-associated infections in clinical settings. This work establishes boronic acid-based nanomaterials as promising candidates for biofilm prevention and antibiotic enhancement, particularly in conditions like cystic fibrosis, where mucin-bacterial interactions contribute to disease progression.

Keywords: Pseudomonas aeruginosa biofilms; antibiofilm materials; boronic acid-functionalized polymers; glycan-binding nanomaterials; mucin interaction; nanoarchitectonics; polyethyleneimine (PEI); synergistic antibiotic activity.

MeSH terms

  • Anti-Bacterial Agents* / chemistry
  • Anti-Bacterial Agents* / pharmacology
  • Bacterial Adhesion* / drug effects
  • Biofilms* / drug effects
  • Boronic Acids* / chemistry
  • Boronic Acids* / pharmacology
  • Humans
  • Microbial Sensitivity Tests
  • Mucins* / chemistry
  • Mucins* / metabolism
  • Polyethyleneimine* / chemistry
  • Polyethyleneimine* / pharmacology
  • Polysaccharides* / chemistry
  • Polysaccharides* / metabolism
  • Pseudomonas aeruginosa* / drug effects
  • Pseudomonas aeruginosa* / physiology

Substances

  • Boronic Acids
  • Anti-Bacterial Agents
  • Polyethyleneimine
  • Mucins
  • benzeneboronic acid
  • Polysaccharides