Deep eutectic solvent-based pretreatment for improved cellulose nanofibrils extraction from sugarcane leaf pulp as bioplastic reinforcers

Int J Biol Macromol. 2025 Aug;319(Pt 2):145485. doi: 10.1016/j.ijbiomac.2025.145485. Epub 2025 Jun 24.

Abstract

Globally, 40 % of fossil-based plastics are used in food packaging, most of which are non-biodegradable, contributing to environmental pollution and potential health risks. This study explores the use of cellulose nanofibrils (CNF) from sugarcane leaf pulp as a reinforcing agent in biodegradable agar-based bioplastics, offering a sustainable alternative. CNF was extracted via deep eutectic solvents (DES) with three molar ratios of choline chloride and oxalic acid dihydrate (1:1, 1:2, 2:1), followed by surface modification. This study achieved a 61.3 % yield with a 1:1 DES ratio, 86.9 % cellulose content, 45.5 % crystallinity, and a thermal degradation temperature (Tdmax) of 334.5 °C. CNF surface modification significantly enhanced the bioplastic's mechanical strength, water resistance, and thermal stability. Additionally, increasing DES-treated CNF concentrations (5 %-25 %) improved bioplastic performance. This optimization not only utilizes agricultural waste but also creates high-quality, eco-friendly bioplastics that align with industrial standards for sustainable packaging solutions.

Keywords: Cellulose nanofibril; Deep eutectic solvent; Sugarcane leaves.

MeSH terms

  • Biodegradable Plastics* / chemistry
  • Cellulose* / chemistry
  • Cellulose* / isolation & purification
  • Deep Eutectic Solvents* / chemistry
  • Nanofibers* / chemistry
  • Plant Leaves* / chemistry
  • Saccharum* / chemistry
  • Solvents / chemistry
  • Temperature

Substances

  • Cellulose
  • Deep Eutectic Solvents
  • Biodegradable Plastics
  • Solvents