Abstract
Nucleotide-bound crystal structures of SARS-CoV-2 NSP13 in ADP- and ATP-bound states were resolved to 1.8 and 1.9 Å, respectively. The ADP-bound model captures a state immediately following ATP hydrolysis, with both ADP and orthophosphate still present in the active site. Further comparative analysis revealed that crystal packing influences NSP13 by stabilizing the nucleotide-binding site, underscoring the importance of accounting for these effects in structure-based drug design targeting NSP13.
Keywords:
ADP-bound structure; ATP-bound structure; COVID-19; NSP13 helicase; SARS-CoV-2; inorganic phosphate; nucleotide-binding sites.
open access.
MeSH terms
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Adenosine Diphosphate* / chemistry
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Adenosine Diphosphate* / metabolism
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Adenosine Triphosphate* / chemistry
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Adenosine Triphosphate* / metabolism
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Binding Sites
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COVID-19 / virology
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Catalytic Domain
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Crystallography, X-Ray
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Humans
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Hydrolysis
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Methyltransferases
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Models, Molecular
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Nucleotides / chemistry
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Nucleotides / metabolism
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Protein Binding
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Protein Conformation
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RNA Helicases* / chemistry
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RNA Helicases* / metabolism
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SARS-CoV-2* / chemistry
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SARS-CoV-2* / enzymology
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Viral Nonstructural Proteins* / chemistry
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Viral Nonstructural Proteins* / genetics
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Viral Nonstructural Proteins* / metabolism
Substances
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Viral Nonstructural Proteins
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Adenosine Diphosphate
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Adenosine Triphosphate
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Nsp13 protein, SARS-CoV
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RNA Helicases
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Nucleotides
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Methyltransferases