Hyaluronic Acid Microplates for Intra-articular Lubrication and Cartilage Protection in Post-traumatic Osteoarthritis

ACS Appl Mater Interfaces. 2025 Nov 5;17(44):60145-60161. doi: 10.1021/acsami.5c11890. Epub 2025 Oct 12.

Abstract

Osteoarthritis (OA) is the most common joint disorder, characterized by a vicious cycle of synovial inflammation and cartilage degradation. Intra-articular injection of hyaluronic acid (HA)-based products, one of the currently available treatments, provides only temporary symptomatic relief without addressing the underlying inflammation. Here, we engineered several configurations of 20 × 5 μm square-shaped HA-based hydrogel microparticles (μHA) by photopolymerizing HA-methacrylate chains within a sacrificial template. The μHA mechano-pharmacological properties were tuned by adjusting the HA concentration, molecular weight, and degree of methacrylation, resulting in microparticles with a Young's modulus ranging from a few tens (30 kPa) to a few hundred (200 kPa) kilopascals; a structure stable for over a month under oxidative stress conditions; and reduced friction in simulated synovial fluids. Under H2O2-induced oxidative conditions, μHA decreased the production of proinflammatory cytokines (IL-6, IL-1β, and TNF-α) in human chondrocytes to basal levels. In a three-dimensional OA cartilage model, μHA reduced glycosaminoglycan release and matrix metalloproteinase-13 activity, demonstrating chondroprotective effects. In a rigorous murine model of early-stage post-traumatic OA, a single intra-articular injection of μHA lowered proinflammatory gene expression in the synovium to basal levels. In summary, μHA offers a drug-free approach to managing OA by enhancing lubrication and reducing inflammation, providing a sustained therapeutic activity over several weeks.

Keywords: anti-inflammatory activity; hyaluronic acid; lubrication; microparticles; osteoarthritis.

MeSH terms

  • Animals
  • Cartilage, Articular* / drug effects
  • Cartilage, Articular* / metabolism
  • Cartilage, Articular* / pathology
  • Chondrocytes / drug effects
  • Chondrocytes / metabolism
  • Cytokines / metabolism
  • Humans
  • Hyaluronic Acid* / chemistry
  • Hyaluronic Acid* / pharmacology
  • Hyaluronic Acid* / therapeutic use
  • Hydrogels / chemistry
  • Injections, Intra-Articular
  • Lubrication
  • Mice
  • Osteoarthritis* / drug therapy
  • Osteoarthritis* / metabolism
  • Osteoarthritis* / pathology

Substances

  • Hyaluronic Acid
  • Hydrogels
  • Cytokines