Electroactive dopamine-functionalized reduced graphene oxide/alginate hydrogel containing thymol/chitosan nanoparticles for advanced antibacterial and bioadhesive wound dressings

Carbohydr Polym. 2026 May 15:380:124960. doi: 10.1016/j.carbpol.2026.124960. Epub 2026 Jan 20.

Abstract

Engineering conductive multifunctional hydrogels, as novel and promising biomaterials, has attracted growing attention in skin tissue engineering and for promoting wound healing. In this study, inspired by recent advances in mussel-inspired chemistry and nanoreinforcement, dopamine-grafted reduced graphene oxide (PDA-rGO) was employed as the main conductive bioadhesive component. Thymol and chitosan nanoparticles were then loaded into the PDA-rGO/alginate hydrogel (Ty/CsNPs@PDA-rGO/Alg), which was synthesized via a simple, Ca2+-mediated radial diffusion crosslinking method to further enhance the antimicrobial activity of the hydrogel. In vitro analysis showed excellent hemocompatibility (hemolysis rates <0.2%), high biocompatibility (>90% cell viability), strong adhesion (∼8.26 kPa), and the highest cell migration rate (∼71.41%) in 3T3 fibroblasts. The hydrogel exhibited valuable mechanical properties, including a compressive strength of 1.03 MPa and a 3.5-fold increase in storage modulus (G') compared to the pristine matrix. The incorporation of Ty/CsNPs into the hydrogel endowed superior antibacterial activity, with inhibition zones of ∼20 mm (S. aureus) and ∼23 mm (E. coli), along with strong antioxidant activity (>80%). Importantly, the developed hydrogel achieved a conductivity of 3.95 mS·cm-1, comparable to that of human skin. Overall, the engineered multifunctional hydrogel demonstrates great potential as a wound dressing, wound monitoring, electrostimulation-assisted therapy, and integration with wearable biosensors.

Keywords: Bactericidal properties; Chitosan nanoparticles; Conductive bioadhesive hydrogel; Cutaneous wound dressing; Graphene oxide.

MeSH terms

  • 3T3 Cells
  • Alginates* / chemistry
  • Animals
  • Anti-Bacterial Agents* / chemistry
  • Anti-Bacterial Agents* / pharmacology
  • Bandages*
  • Biocompatible Materials / chemistry
  • Biocompatible Materials / pharmacology
  • Cell Survival / drug effects
  • Chitosan* / chemistry
  • Chitosan* / pharmacology
  • Dopamine* / chemistry
  • Escherichia coli / drug effects
  • Graphite* / chemistry
  • Humans
  • Hydrogels* / chemistry
  • Hydrogels* / pharmacology
  • Mice
  • Nanoparticles* / chemistry
  • Staphylococcus aureus / drug effects
  • Thymol* / chemistry
  • Thymol* / pharmacology
  • Wound Healing / drug effects

Substances

  • Graphite
  • Chitosan
  • Alginates
  • Anti-Bacterial Agents
  • Hydrogels
  • Thymol
  • graphene oxide
  • Dopamine
  • Biocompatible Materials