Changes in the protonation state of bacterio-opsin during reconstitution of bacteriorhodopsin

Biophys J. 1980 Jul;31(1):139-45. doi: 10.1016/S0006-3495(80)85045-4.

Abstract

Protonation changes of the protein occur during the reconstitution of bacteriorhodopsin from bacterio-opsin and all-trans retinal in the purple membrane of Halobacterium halobium. The protonation changes are conveniently determined from measures of the pH changes after photoisomerisation of 9-cis retinal in apomembrane preparations, which induces the reconstitution. In addition, to the omega-amino group of the lysine which is involved in the condensation of retinal and bacterio-opsin, the dissociation equilibria of at least two other amino acid residues are changed during the reconstitution. The results are consistent with a proposed model of chromophore structure in which an interaction of the Schiff's base occurs with two protonable amino acid residues.

Publication types

  • Research Support, Non-U.S. Gov't

MeSH terms

  • Apoproteins
  • Bacteriorhodopsins* / radiation effects
  • Carotenoids* / radiation effects
  • Chemical Phenomena
  • Chemistry
  • Diterpenes
  • Halobacterium
  • Hydrogen-Ion Concentration
  • Isomerism
  • Light
  • Models, Chemical
  • Protons
  • Retinaldehyde* / radiation effects
  • Ultraviolet Rays
  • Vitamin A* / analogs & derivatives

Substances

  • Apoproteins
  • Diterpenes
  • Protons
  • Vitamin A
  • Carotenoids
  • 13-cis-retinal
  • 9-cis-retinal
  • Bacteriorhodopsins
  • bacterio-opsin
  • Retinaldehyde