Phage T4 DNA [N6-adenine]methyltransferase. Overexpression, purification, and characterization

J Biol Chem. 1995 Jun 16;270(24):14389-93. doi: 10.1074/jbc.270.24.14389.

Abstract

The bacteriophage T4 dam gene, encoding the Dam DNA [N6-adenine]methyltransferase (MTase), has been subcloned into the plasmid expression vector, pJW2. In this construct, designated pINT4dam, transcription is from the regulatable phage lambda pR and pL promoters, arranged in tandem. A two-step purification scheme using DEAE-cellulose and phosphocellulose columns in series, followed by hydroxyapatite chromatography, was developed to purify the enzyme to near homogeneity. The yield of purified protein was 2 mg/g of cell paste. The MTase has an s20,w of 3.0 S and a Stokes radius of 23 A and exists in solution as a monomer. The Km for the methyl donor, S-adenosylmethionine, is 0.1 x 10(-6) M, and the Km for substrate nonglucosylated, unmethylated T4 gt- dam DNA is 1.1 x 10(-12) M. The products of DNA methylation, S-adenosyl-L-homocysteine and methylated DNA, are competitive inhibitors of the reaction; Ki values of 2.4 x 10(-6) M and 4.6 x 10(-12) M, respectively, were observed. T4 Dam methylates the palindromic tetranucleotide, GATC, designated the canonical sequence. However, at high MTase:DNA ratios, T4 Dam can methylate some noncanonical sequences belonging to GAY (where Y represents cytosine or thymine).

Publication types

  • Research Support, U.S. Gov't, P.H.S.

MeSH terms

  • Chromatography, DEAE-Cellulose
  • Chromatography, Gel
  • Cloning, Molecular
  • Electrophoresis, Polyacrylamide Gel
  • Escherichia coli / genetics
  • Escherichia coli Proteins
  • Kinetics
  • Methylation
  • Methyltransferases / genetics*
  • Methyltransferases / isolation & purification
  • Methyltransferases / metabolism
  • Molecular Weight
  • Plasmids
  • Site-Specific DNA-Methyltransferase (Adenine-Specific)*
  • Viral Proteins

Substances

  • Escherichia coli Proteins
  • Viral Proteins
  • Methyltransferases
  • Dam methyltransferase
  • Site-Specific DNA-Methyltransferase (Adenine-Specific)
  • dam protein, Bacteriophage T4
  • dam protein, E coli